Michigan Center for Materials Characterization > Techniques and Instruments > JEOL 2010F Analytical Electron Microscope

JEOL 2010F Analytical Electron Microscope

Applications

  • Conventional BF/DF-TEM, SAED, and HRTEM imaging
  • In-situ heating and cooling
  • In-situ tensile and compression

Contact

Haiping Sun

Location

Room G020

Acknowledgments

Publications, presentations, and posters resulting from work on this instrument should state: “The authors acknowledge the financial support of the University of Michigan College of Engineering and NSF grant #DMR-9871177, and technical support from the Michigan Center for Materials Characterization.“

Specifications

  • Accelerating Voltage: 200 kV
  • Filament: Zirconated Tungsten (100) thermal field emission tip
  • Vacuum: ~1.5 x10-7 torr
  • Resolution
    • CTEM 0.10 nm lattice / 0.25 nm point-to-point
    • STEM 0.17 nm HAADF (high angle annular dark field)
  • XEDS System
    • Horizontal Ultra-thin Window Si-Li X-ray detector (active area = 30 mm2) capable of detecting elements with Z >5.
    • EDAX r-TEM Detector with EDAX acquisition software
  • Image Acquisition & Analysis System
    • Gatan #794 cooled multi-scan CCD TV camera for high resolution imaging (above the GIF)
    • Gatan #692 Retractable TV rate CCD TV camera.
  • Sample Holders
    • JEOL Single-Tilt Stage
    • JEOL Double-Tilt Analytical Stage
    • Gatan #646 Double-Tilt (x=±35 degrees, y=±35 degrees) Low Background (Be) Stage with Faraday cup.
    • Gatan #636 Double-Tilt (x=±35 degrees, y=±35 degrees) Low Background (Be) Liquid-Nitrogen Stage.
    • Gatan #652 Double-Tilt Heating Holder with a maximum operating temperature of 1000 degrees Celsius.
    • Hysitron PI-95 pico-indenter
  • Other Accessories
    • Free lens control, fully independent control of all lenses.
    • FasTEM remote NT server based control system.

References

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  10. The Role of Co-injected Helium on Swelling and Cavity Evolution at High Damage Levels in Ferritic-Martensitic Steels, D. Woodley, S. Taller, Z. Jiao, K. Sun, G.S. Was, Journal of Nuclear Materials, 550, 152912, 2021
  11. Predicting Structural Material Degradation in Advanced Nuclear Reactors with Ion Irradiation, S. Taller, G. VanCoevering, B.D. Wirth, G.S. Was, Scientific Reports, 11, 2949, 2021
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  15. Understanding Bubble and Void Nucleation in Dual Ion Irradiated T91 Steel using Single Parameter Experiments, S. Taller, G.S. Was, Acta Materialia, 198, 47-60, 2020
  16. Developing of Nano Sized Fibrous Eutectic Silicon in Hypereutectic Al–Si Alloy by Laser Remelting, J. Abboud, J. Mazumder, Scientific Reports, 10, 12090, 2020
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  20. Multi-Step Crystallization of Self-Organized Spiral Eutectics, S. Moniri, H. Bale, T. Volkenandt, Y. Wang, J. Gao, T. Lu, K. Sun, R.O. Richie, A.J. Shahani, Small, 1906146, 2020
  21. Energy Transport in CsPbBr3 Perovskite Nanocrystal Solids, M. Yang, P. Moroz, E. Miller, D. Porotnikov, J. Cassidy, C. Ellison, X. Medvedeva, A. Klinkova, M. Zamkov, ACS Photonics, 7(1), 154-164, 2020
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  35. Indium-Doped Co3O4 Nanorods for Catalytic Oxidation of CO and C3H6 towards Diesel Exhaust, L. Ma, C.Y. Seo, X.Y. Chen, K. Sun, J.W. Schwank, Applied Catalysis B – Environmental, 222, 44-58, 2017
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  38. Optical Anisotropy and Sign Reversal in Layer-by-Layer Assembled Films from Chiral Nanoparticles, Z. Liang, K. Bernardino, J. Han, Y. Zhou, K. Sun, A.F. de Moura, N.A. Kotov, Faraday Discussions, 191, 141-157, 2016
  39. Direct Observation of Hydrogenation and Dehydrogenation of a Zirconium Alloy. H.H. Shen, X.T. Zu, B. Chen, C.Q. Huang, K. Sun. Journal of Alloys and Compounds, 659, 23-30, 2016
  40. Void Swelling and Microstructure Evolution at Very High Damage Levels in Self-Ion Irradiated Ferritic-Martensitic Steels, E. Getto, K. Sun, A.M. Monterrosa, Z. Jiao, M.J. Hackett, G.S. Was, Journal of Nuclear Materials,  480, 159-176, 2016
  41. Methodology for Determining Void Swelling at Very High Damage under Ion Irradiation, E. Getto, K. Sun, S. Taller, A.M. Monterrosa, Z. Jiao, G.S. Was, Journal of Nuclear Materials,  477, 273-279, 2016
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  44. Linking the Microstructure of a Heat-Treated WE43 Mg Alloy with its Corrosion Behavior, P-W. Chou, E.A. Marquis, Corrosion Science, 101, 94-104, 2015
  45. Hierarchical ZnO Nanowire Growth with Tunable Orientations on Versatile Substrates Using Atomic Layer Deposition Seeding, A.R. Bielinski, E. Kazyak, C.M. Schlepütz, H.J. Jung, K.N. Wood, N.P. Dasgupta, Chem. Mater., 27(13), 4799–4807, 2015
  46. Formation and Evolution of Ripples on Ion-Irradiated Semiconductor Surfaces, M. Kang, J.H. Wu, W. Ye, Y. Jiang, E.A. Robb, C. Chen, R. S. Goldman, Appl. Phys. Lett., 104, 052103, 2014
  47. Direct Fabrication of Graphene on SiO2 Enabled by Thin Film Stress Engineering, D.Q. McNerny, B. Viswanath, D. Copic, F.R. Laye, C. Prohoda, A.C. Brieland-Shoultz, E.S. Polsen, N.T. Dee, V.S. Veerasamy, A.J. Hart, Scientific Reports, 4, 5049, 2014
  48. The Mechanism of Radiation-Induced Segregation in Ferritic-Martensitic Alloys, P. Wharry, G.S. Was, Acta Mater. , 65, 42-55, 2014