Applications
- Conventional BF/DF-TEM, SAED, and HRTEM imaging
- In-situ heating and cooling
- In-situ tensile and compression
Contact
Location
Room G020
Acknowledgments
Publications, presentations, and posters resulting from work on this instrument should state: “The authors acknowledge the financial support of the University of Michigan College of Engineering and NSF grant #DMR-9871177, and technical support from the Michigan Center for Materials Characterization.“
Specifications
- Accelerating Voltage: 200 kV
- Filament: Zirconated Tungsten (100) thermal field emission tip
- Vacuum: ~1.5 x10-7 torr
- Resolution
- CTEM 0.10 nm lattice / 0.25 nm point-to-point
- STEM 0.17 nm HAADF (high angle annular dark field)
- XEDS System
- Horizontal Ultra-thin Window Si-Li X-ray detector (active area = 30 mm2) capable of detecting elements with Z >5.
- EDAX r-TEM Detector with EDAX acquisition software
- Image Acquisition & Analysis System
- Sample Holders
- JEOL Single-Tilt Stage
- JEOL Double-Tilt Analytical Stage
- Gatan #646 Double-Tilt (x=±35 degrees, y=±35 degrees) Low Background (Be) Stage with Faraday cup.
- Gatan #636 Double-Tilt (x=±35 degrees, y=±35 degrees) Low Background (Be) Liquid-Nitrogen Stage.
- Gatan #652 Double-Tilt Heating Holder with a maximum operating temperature of 1000 degrees Celsius.
- Hysitron PI-95 pico-indenter
- Other Accessories
- Free lens control, fully independent control of all lenses.
- FasTEM remote NT server based control system.
References and Publications
- Chiral Nanoceramics, J. Fan, N.A. Kotov, Advanced Materials, 201906738, 2020
- Emergence of Complexity in Hierarchically Organized Chiral Particles, W. Jiang, Z-b. Qu, P. Kumar, D. Vecchio, Y. Wang, Y. Ma, J.H. Bahng, K. Bernardino, W.R. Gomes, F.M. Colombari, A. Lozada-Blanco, M. Veksler, E. Marino, A. Simon, C. Murray, S.R. Muniz, A.F. de Moura, N.A. Kotov, Science, 368, 642-648, 2020
- In-Situ Transmission Electron Microscopy (TEM) Measurements of Ge Nanowire Synthesis with Liquid Metal Nanodroplets in Water, Q. Cheek, E. Fahrenkrug, S. Hlynchuk, D. Hein Alsem, N.J. Salmon, S. Maldonado, ACS Nano, 14(3), 2869-2879, 2020
- Multi-Step Crystallization of Self-Organized Spiral Eutectics, S. Moniri, H. Bale, T. Volkenandt, Y. Wang, J. Gao, T. Lu, K. Sun, R.O. Richie, A.J. Shahani, Small, 1906146, 2020
- Energy Transport in CsPbBr3 Perovskite Nanocrystal Solids, M. Yang, P. Moroz, E. Miller, D. Porotnikov, J. Cassidy, C. Ellison, X. Medvedeva, A. Klinkova, M. Zamkov, ACS Photonics, 7(1), 154-164, 2020
- Nanoscale Deformation Mechanics Reveal Resilience in Nacre of Pinna Nobilis Shell, J. Gim, N. Schnitzer, L.M. Otter, Y. Cui, S. Motreuil, F. Marin, S.E. Wolf, D.E. Jacob, A. Misra, R. Hovden, Nature Communications, 10, 4822, 2019
- Dislocation Pile-Ups at β1 Precipitate Interfaces in Mg-Rare Earth (RE) Alloys, Z. Huang, C. Yang, L. Qi, J.E. Allison, A. Misra, Materials Science & Engineering A, 742, 278-286, 2019
- Emulation of Fast Reactor Irradiated T91 using Dual Ion Beam Irradiation, S. Taller, Z. Jiao, K. Field, G.S. Was, Journal of Nuclear Materials, 527, 151831, 2019
- Oxide Growth and Dissolution on 316L Stainless Steel during Irradiation in High Temperature Water, R.D. Hanbury, G.S. Was, Corrosion Science, 157, 305-311, 2019
- Micro- and Nano-Scale Intermetallic Phases in AA2070-T8 and their Corrosion Behavior, Y. Zhu, K. Sun, J. Garves, L.G. Bland, J. Locke, J. Allison, G.S. Frankel, Electrochimica Acta, 319, 634-648, 2019
- Annealing Induced Interfacial Evolution of Titanium/Gold Metallization on Unintentionally Doped β-Ga2O3, M. Lee, R.L. Peterson, ECS Journal of Solid State Science and Technology, 8(7), Q3176-Q3179, 2019
- Interfacial Reactions of Titanium/Gold Ohmic Contacts with Sn-Doped β-Ga2O3, M. Lee, R.L. Peterson, APL Materials, 7(2), 022524, 2019
- Suppression of Shear Banding in High-Strength Cu/Mo Nanocomposites with Hierarchical Bicontinuous Intertwined Structures, Y. Cui, B. Derby, N. Li, N.A. Mara, A. Misra, Materials Research Letters, 6(3), 184-190, 2018
- Self-Ion Emulation of High Dose Neutron Irradiated Microstructure in Stainless Steels, Z. Jiao, J. Michalika, G.S. Was, Journal of Nuclear Materials, 501, 312-318, 2018
- Early Oxidation Behavior of Si-Coated Titanium, K. Chou, P. Chu, E.A. Marquis, Corrosion Science, 140, 297-306, 2018
- Intermetallic Phases in Aluminum Alloys and Their Roles in Localized Corrosion, Y. Zhu, K. Sun, G.S. Frankel, Journal of the Electrochemical Society, 165(11), C807-C820, 2018
- Intergranular Li Metal Propagation through Polycrystalline Li6.25Al0.25La3Zr2O12 Ceramic Electrolyte, E.J. Cheng, A. Sharafi, J. Sakamoto, Electrochimica Acta, 85-91, 223, 2017
- He+ Irradiation Induced Cracking and Exfoliating on the Surface of Ti3AlC2 , H.H. Shen, F.Z. Li, H.B. Zhang, S.M. Peng, K. Sun, X.T. Zu, L. Ao, Journal of Nuclear Materials, 485, 262-272, 2017
- Indium-Doped Co3O4 Nanorods for Catalytic Oxidation of CO and C3H6 towards Diesel Exhaust, L. Ma, C.Y. Seo, X.Y. Chen, K. Sun, J.W. Schwank, Applied Catalysis B – Environmental, 222, 44-58, 2017
- The Co-Evolution of Microstructure Features in Self-Ion Irradiated HT9 at Very High Damage Levels, E. Getto, G. Vancoevering, G.S. Was, Journal of Nuclear Materials, 484, 193-208, 2017
- Biomimetic Hierarchical Assembly of Helical Supraparticles from Chiral Nanoparticles. Y.L. Zhou, R.L. Marson, G. van Anders, J. Zhu, G. Ma, P. Ercius, K. Sun, B. Yeom, S.C. Glotzer, and N.A. Kotov, ACS Nano, 10(3), 3248-3256, 2016
- Optical Anisotropy and Sign Reversal in Layer-by-Layer Assembled Films from Chiral Nanoparticles, Z. Liang, K. Bernardino, J. Han, Y. Zhou, K. Sun, A.F. de Moura, N.A. Kotov, Faraday Discussions, 191, 141-157, 2016
- Direct Observation of Hydrogenation and Dehydrogenation of a Zirconium Alloy. H.H. Shen, X.T. Zu, B. Chen, C.Q. Huang, K. Sun. Journal of Alloys and Compounds, 659, 23-30, 2016
- Void Swelling and Microstructure Evolution at Very High Damage Levels in Self-Ion Irradiated Ferritic-Martensitic Steels, E. Getto, K. Sun, A.M. Monterrosa, Z. Jiao, M.J. Hackett, G.S. Was, Journal of Nuclear Materials, 480, 159-176, 2016
- Methodology for Determining Void Swelling at Very High Damage under Ion Irradiation, E. Getto, K. Sun, S. Taller, A.M. Monterrosa, Z. Jiao, G.S. Was, Journal of Nuclear Materials, 477, 273-279, 2016
- Formation and Coarsening of Near-Surface Ga Nanoparticles on SiNx , J.C. Canniff, S. Jeon, R.S. Goldman, Appl. Phys. Lett., 106, 243102, 2015
- Exposing the Sub-Surface of Historical Daguerreotypes and the Effects of Sulfur-Induced Corrosion, E.A. Marquis, Y. Chen, J. Kohanek, Y. Dong, S. Centeno, Corrosion Science, 94, 438-444, 2015
- Linking the Microstructure of a Heat-Treated WE43 Mg Alloy with its Corrosion Behavior, P-W. Chou, E.A. Marquis, Corrosion Science, 101, 94-104, 2015
- Hierarchical ZnO Nanowire Growth with Tunable Orientations on Versatile Substrates Using Atomic Layer Deposition Seeding, A.R. Bielinski, E. Kazyak, C.M. Schlepütz, H.J. Jung, K.N. Wood, N.P. Dasgupta, Chem. Mater., 27(13), 4799–4807, 2015
- Formation and Evolution of Ripples on Ion-Irradiated Semiconductor Surfaces, M. Kang, J.H. Wu, W. Ye, Y. Jiang, E.A. Robb, C. Chen, R. S. Goldman, Appl. Phys. Lett., 104, 052103, 2014
- Direct Fabrication of Graphene on SiO2 Enabled by Thin Film Stress Engineering, D.Q. McNerny, B. Viswanath, D. Copic, F.R. Laye, C. Prohoda, A.C. Brieland-Shoultz, E.S. Polsen, N.T. Dee, V.S. Veerasamy, A.J. Hart, Scientific Reports, 4, 5049, 2014
- The Mechanism of Radiation-Induced Segregation in Ferritic-Martensitic Alloys, P. Wharry, G.S. Was, Acta Mater. , 65, 42-55, 2014