JEOL 2010F Analytical Electron Microscope

Applications

  • STEM imaging
  • Chemical mapping
  • In-situ imaging

Contact

Haiping Sun

Location

Room G020

Acknowledgments

Publications, presentations, and posters resulting from work on this instrument should state: “The authors acknowledge the financial support of the University of Michigan College of Engineering and NSF grant #DMR-9871177, and technical support from the Michigan Center for Materials Characterization.“

Specifications

  • Accelerating Voltage: 0 to 200 kV (50 V steps)
  • Filament: Zirconated Tungsten (100) thermal field emission tip
  • Vacuum: ~1.5 x10-7 torr
  • Resolution
    • CTEM 0.10 nm lattice / 0.25 nm point-to-point
    • STEM 0.17 nm HAADF (high angle annular dark field)
  • XEDS System
    • Horizontal Ultra-thin Window Si-Li X-ray detector (active area = 30 mm2) capable of detecting elements with Z >5.
    • EDAX r-TEM Detector with EDAX acquisition software
  • Image Acquisition & Analysis System
    • Gatan #794 cooled multi-scan CCD TV camera for high resolution imaging (above the GIF)
    • Gatan #692 Retractable TV rate CCD TV camera.
  • Sample Holders
    • JEOL Single-Tilt Stage
    • JEOL Double-Tilt Analytical Stage
    • Gatan #646 Double-Tilt (x=±35 degrees, y=±35 degrees) Low Background (Be) Stage with Faraday cup.
    • Gatan #636 Double-Tilt (x=±35 degrees, y=±35 degrees) Low Background (Be) Liquid-Nitrogen Stage.
    • Gatan #652 Double-Tilt Heating Holder with a maximum operating temperature of 1000 degrees Celsius.
  • Other Accessories
    • Free lens control, fully independent control of all lenses.
    • FasTEM remote NT server based control system.

References and Publications

  1. Chiral Nanoceramics, J. Fan, N.A. Kotov, Advanced Materials, 201906738, 2020
  2. Emergence of Complexity in Hierarchically Organized Chiral Particles, W. Jiang, Z-b. Qu, P. Kumar, D. Vecchio, Y. Wang, Y. Ma, J.H. Bahng, K. Bernardino, W.R. Gomes, F.M. Colombari, A. Lozada-Blanco, M. Veksler, E. Marino, A. Simon, C. Murray, S.R. Muniz, A.F. de Moura, N.A. Kotov, Science, 368, 642-648, 2020
  3. In-Situ Transmission Electron Microscopy (TEM) Measurements of Ge Nanowire Synthesis with Liquid Metal Nanodroplets in Water, Q. Cheek, E. Fahrenkrug, S. Hlynchuk, D. Hein Alsem, N.J. Salmon, S. Maldonado, ACS Nano, 14(3), 2869-2879, 2020
  4. Multi-Step Crystallization of Self-Organized Spiral Eutectics, S. Moniri, H. Bale, T. Volkenandt, Y. Wang, J. Gao, T. Lu, K. Sun, R.O. Richie, A.J. Shahani, Small, 1906146, 2020
  5. Energy Transport in CsPbBr3 Perovskite Nanocrystal Solids, M. Yang, P. Moroz, E. Miller, D. Porotnikov, J. Cassidy, C. Ellison, X. Medvedeva, A. Klinkova, M. Zamkov, ACS Photonics, 7(1), 154-164, 2020
  6. Nanoscale Deformation Mechanics Reveal Resilience in Nacre of Pinna Nobilis Shell, J. Gim, N. Schnitzer, L.M. Otter, Y. Cui, S. Motreuil, F. Marin, S.E. Wolf, D.E. Jacob, A. Misra, R. Hovden, Nature Communications, 10, 4822, 2019
  7. Dislocation Pile-Ups at β1 Precipitate Interfaces in Mg-Rare Earth (RE) Alloys, Z. Huang, C. Yang, L. Qi, J.E. Allison, A. Misra, Materials Science & Engineering A, 742, 278-286, 2019
  8. Emulation of Fast Reactor Irradiated T91 using Dual Ion Beam Irradiation, S. Taller, Z. Jiao, K. Field, G.S. Was, Journal of Nuclear Materials, 527, 151831, 2019 
  9. Oxide Growth and Dissolution on 316L Stainless Steel during Irradiation in High Temperature Water, R.D. Hanbury, G.S. Was, Corrosion Science, 157, 305-311, 2019
  10. Micro- and Nano-Scale Intermetallic Phases in AA2070-T8 and their Corrosion Behavior, Y. Zhu, K. Sun, J. Garves, L.G. Bland, J. Locke, J. Allison, G.S. Frankel, Electrochimica Acta, 319, 634-648, 2019 
  11. Annealing Induced Interfacial Evolution of Titanium/Gold Metallization on Unintentionally Doped β-Ga2O3, M. Lee, R.L. Peterson, ECS Journal of Solid State Science and Technology, 8(7), Q3176-Q3179, 2019
  12. Interfacial Reactions of Titanium/Gold Ohmic Contacts with Sn-Doped β-Ga2O3, M. Lee, R.L. Peterson, APL Materials, 7(2), 022524, 2019
  13. Suppression of Shear Banding in High-Strength Cu/Mo Nanocomposites with Hierarchical Bicontinuous Intertwined Structures, Y. Cui, B. Derby, N. Li, N.A. Mara, A. Misra, Materials Research Letters, 6(3), 184-190, 2018
  14. Self-Ion Emulation of High Dose Neutron Irradiated Microstructure in Stainless Steels, Z. Jiao, J. Michalika, G.S. Was, Journal of Nuclear Materials, 501, 312-318, 2018
  15. Early Oxidation Behavior of Si-Coated Titanium, K. Chou, P. Chu, E.A. Marquis, Corrosion Science, 140, 297-306, 2018
  16. Intermetallic Phases in Aluminum Alloys and Their Roles in Localized Corrosion, Y. Zhu, K. Sun, G.S. Frankel, Journal of the Electrochemical Society, 165(11), C807-C820, 2018
  17. Intergranular Li Metal Propagation through Polycrystalline Li6.25Al0.25La3Zr2O12 Ceramic Electrolyte, E.J. Cheng, A. Sharafi, J. Sakamoto, Electrochimica Acta, 85-91, 223, 2017
  18. He+ Irradiation Induced Cracking and Exfoliating on the Surface of Ti3AlC2 , H.H. Shen, F.Z. Li, H.B. Zhang, S.M. Peng, K. Sun, X.T. Zu, L. Ao, Journal of Nuclear Materials,  485, 262-272, 2017
  19. Indium-Doped Co3O4 Nanorods for Catalytic Oxidation of CO and C3H6 towards Diesel Exhaust, L. Ma, C.Y. Seo, X.Y. Chen, K. Sun, J.W. Schwank, Applied Catalysis B – Environmental, 222, 44-58, 2017
  20. The Co-Evolution of Microstructure Features in Self-Ion Irradiated HT9 at Very High Damage Levels, E. Getto, G. Vancoevering, G.S. Was, Journal of Nuclear Materials, 484, 193-208, 2017
  21. Biomimetic Hierarchical Assembly of Helical Supraparticles from Chiral Nanoparticles. Y.L. Zhou, R.L. Marson, G. van Anders, J. Zhu, G. Ma, P. Ercius, K. Sun, B. Yeom, S.C. Glotzer, and N.A. Kotov, ACS Nano, 10(3), 3248-3256, 2016
  22. Optical Anisotropy and Sign Reversal in Layer-by-Layer Assembled Films from Chiral Nanoparticles, Z. Liang, K. Bernardino, J. Han, Y. Zhou, K. Sun, A.F. de Moura, N.A. Kotov, Faraday Discussions, 191, 141-157, 2016
  23. Direct Observation of Hydrogenation and Dehydrogenation of a Zirconium Alloy. H.H. Shen, X.T. Zu, B. Chen, C.Q. Huang, K. Sun. Journal of Alloys and Compounds, 659, 23-30, 2016
  24. Void Swelling and Microstructure Evolution at Very High Damage Levels in Self-Ion Irradiated Ferritic-Martensitic Steels, E. Getto, K. Sun, A.M. Monterrosa, Z. Jiao, M.J. Hackett, G.S. Was, Journal of Nuclear Materials,  480, 159-176, 2016
  25. Methodology for Determining Void Swelling at Very High Damage under Ion Irradiation, E. Getto, K. Sun, S. Taller, A.M. Monterrosa, Z. Jiao, G.S. Was, Journal of Nuclear Materials,  477, 273-279, 2016
  26. Formation and Coarsening of Near-Surface Ga Nanoparticles on SiNx , J.C. Canniff, S. Jeon, R.S. Goldman, Appl. Phys. Lett., 106, 243102, 2015
  27. Exposing the Sub-Surface of Historical Daguerreotypes and the Effects of Sulfur-Induced Corrosion, E.A. Marquis, Y. Chen, J. Kohanek, Y. Dong, S. Centeno, Corrosion Science, 94, 438-444, 2015 
  28. Linking the Microstructure of a Heat-Treated WE43 Mg Alloy with its Corrosion Behavior, P-W. Chou, E.A. Marquis, Corrosion Science, 101, 94-104, 2015
  29. Hierarchical ZnO Nanowire Growth with Tunable Orientations on Versatile Substrates Using Atomic Layer Deposition Seeding, A.R. Bielinski, E. Kazyak, C.M. Schlepütz, H.J. Jung, K.N. Wood, N.P. Dasgupta, Chem. Mater., 27(13), 4799–4807, 2015
  30. Formation and Evolution of Ripples on Ion-Irradiated Semiconductor Surfaces, M. Kang, J.H. Wu, W. Ye, Y. Jiang, E.A. Robb, C. Chen, R. S. Goldman, Appl. Phys. Lett., 104, 052103, 2014
  31. Direct Fabrication of Graphene on SiO2 Enabled by Thin Film Stress Engineering, D.Q. McNerny, B. Viswanath, D. Copic, F.R. Laye, C. Prohoda, A.C. Brieland-Shoultz, E.S. Polsen, N.T. Dee, V.S. Veerasamy, A.J. Hart, Scientific Reports, 4, 5049, 2014
  32. The Mechanism of Radiation-Induced Segregation in Ferritic-Martensitic Alloys, P. Wharry, G.S. Was, Acta Mater. , 65, 42-55, 2014