JEOL 3100R05

Applications

  • Atomic structure
  • Atomic chemical mapping
  • In-situ imaging (deformation, gas, liquid, temperature)

Contact

Tao Ma

Location

Room G026 (Microscope) and G028 (Control Room)

Acknowledgments

Publications, presentations, and posters resulting from work on this instrument should state: “The authors acknowledge the financial support of the University of Michigan College of Engineering and NSF grant #DMR-0723032, and technical support from the Michigan Center for Materials Characterization.“

Specifications

  • Accelerating Voltage
    • 80, 200 and 300kV 
  • Filament
    • Tungsten cold field emission tip
  • Vacuum
    • Gun ~1.0 x 10-9 torr
    • Column ~1.0 x 10-7 torr
  • Resolution
    • CTEM 0.055 nm point-to-point
    • STEM 0.055 nm point-to-point
  • XEDS System
    • Horizontal Ultra-thin Window JEOL SDD X-ray detector (active area = 60 mm2) capable of detecting elements with Z >5.
  • EELS System
    • Gatan #965 Quantum Imaging Filter (GIF) for electron energy loss spectroscopy and imaging.
  • Image Acquisition & Analysis System
    • Gatan Ultrascan 1000 CCD TV camera for high resolution imaging (above the GIF)
  • Compatible sample Holders
    • JEOL Single-Tilt Stage
    • JEOL Double-Tilt Analytical Stage
    • Gatan #646 Double-Tilt (x=±35 degrees, y=±35 degrees) Low Background (Be) Stage with Faraday cup.
    • Gatan #636 Double-Tilt (x=±35 degrees, y=±35 degrees) Low Background (Be) Liquid-Nitrogen Stage.
    • Gatan #652 Double-Tilt Heating Holder with a maximum operating temperature of 1000 degrees Celsius.
  • In-situ holders 
    • Hysitron pico-indenter
  • Other Accessories
    • Free lens control, fully independent control of all lenses.
    • TEMCon PC control software.
    • JEOL Cs Correctors for STEM and TEM 

References and Publications

  1. Multi-Step Crystallization of Self-Organized Spiral Eutectics, S. Moniri, H. Bale, T. Volkenandt, Y. Wang, J. Gao, T. Lu, K. Sun, R.O. Richie, A.J. Shahani, Small, 1906146, 2020
  2. Performance Characteristics of AlGaN Tunnel Junction Light Emitting Diodes, A. Pandey, W. Shin, R. Hovden, Z. Mi, Photonics Research, 8(3), 331-337, 2020
  3. Self-Assembly of Chiral Nanoparticles into Semiconductor Helices with Tunable Near-Infrared Optical Activity, J. Yan, W. Feng, J-Y. Kim, J. Lu, P. Kumar, Z. Mu, X. Wu, X. Mao, N.A. Kotov, Chem. Mater., 32(1), 476-488, 2020 
  4. Monolayer GaN Excitonic Deep Ultraviolet Light Emitting Diodes, Y. Wu, X. Liu, P. Wang, D.A. Laleyan, K. Sun, Y. Sun, C. Ahn, M. Kira, E. Kioupakis, Z. Mi, Appl. Phys. Lett, 116, 013101, 2020 
  5. Monolithic Integration of High-Voltage Thin-Film Electronics on Low-Voltage Integrated Circuits Using a Solution Process, Y. Son, B. Frost, Y. Zhao, R.L. Peterson, Nature Electronics, 2, 540-548, 2019
  6. Influence of Metal Nanocomposite Morphology on Helium Implantation Response, B.K. Derby, J.K. Baldwin, Y. Wang, M.J. Demkowicz, A. Misra, N. Li, Scripta Materialia, 177, 229-233, 2019
  7. Faceted He-Filled “Pancakes” Confined within Nanoscale Metal Layers, B.K. Derby, J.K. Baldwin, D. Chen, M.J. Demkowicz, Y.Q. Wang, A. Misra, N. Li, JOM, 1-5, 2019
  8. Nanoscale Deformation Mechanics Reveal Resilience in Nacre of Pinna Nobilis Shell, J. Gim, N. Schnitzer, L.M. Otter, Y. Cui, S. Motreuil, F. Marin, S.E. Wolf, D.E. Jacob, A. Misra, R. Hovden, Nature Communications, 10, 4822, 2019
  9. A Single-Junction Cathodic Approach for Stable Unassisted Solar Water Splitting, Y. Wang, Y. Wu, J. Schwartz, S. Sung, R. Hovden, Z. Mi, Joule, 3(10), 2444-2456, 2019 
  10. Tuning Catalytic Performance by Controlling Reconstruction Process in Operando Condition, C. Cai, S. Han, K. Sun, L. Qiao, S. Li, X. Zu, Applied Catalysis B: Environmental, 260, 118103, 2019
  11. Stable Unassisted Solar Water Splitting on Semiconductor Photocathodes Protected by Multi-Functional GaN Nanostructures, Y. Wang, J. Schwartz, J. Gim, R. Hovden, Z. Mi, ACS Energy Letters, 4, 1541-1548, 2019
  12. A Quadruple-Band Metal-Nitride Nanowire Artificial Photosynthesis System for High Efficiency Photocatalytic Overall Solar Water Splitting, Y. Wang, Y. Wu, K. Sun, Z. Mi, Materials Horizons, 2019
  13. Stability and Strain-Driven Evolution of β′ Precipitate in Mg-Y Alloys, E.L.S. Solomon, A.R. Natarajan, A.M. Roy, V. Sundararaghavan, A. Van der Ven, E.A. Marquis, Acta Materialia, 166, 148-157, 2019
  14. Design of Bicontinuous Metallic Nanocomposites for High-Strength and Plasticity, Y. Cui, B. Derby, N. Li, A. Misra, Materials Design, 166, 107602, 2019
  15. Dislocation Pile-Ups at β1 Precipitate Interfaces in Mg-Rare Earth (RE) Alloys, Z. Huang, C. Yang, L. Qi, J.E. Allison, A. Misra, Materials Science & Engineering A, 742, 278-286, 2019
  16. An In0.42Ga0.58N Tunnel Junction Nanowire Photocathode Monolithically Integrated on a Nonplanar Si Wafer, Y. Wang, S. Vanka, J. Gim, Y. Wu, R. Fan, Y. Zhang, J. Shi, M. Shen, R. Hovden, Z. Mi, Nano Energy, 57, 405-413, 2019
  17. Optical and Interface Characteristics of Al0.56Ga0.44N/Al0.62Ga0.38N Multiquantum Wells with ∼280 nm Emission Grown by Plasma-Assisted Molecular Beam Epitaxy, Journal of Crystal Growth, 508, 66-71, 2019
  18. Processing of Novel Pseudomorphic Cu–Mo Hierarchies in Thin Films, B. Derby, Y. Cui, J. Baldwin, R. Arróyave, M.J. Demkowicz, A. Misra, Materials Research Letters, 7(1), 1-11, 2018
  19. Suppression of Shear Banding in High-Strength Cu/Mo Nanocomposites with Hierarchical Bicontinuous Intertwined Structures, Y. Cui, B. Derby, N. Li, N.A. Mara, A. Misra, Materials Research Letters, 6(3), 184-190, 2018
  20. Surfactant-Induced Chemical Ordering of GaAsN:Bi, J. Occena, T. Jen, H. Lu, B.A. Carter, T.S. Jimson, A.G. Norman, R.S. Goldman, Applied Physics Letters, 113, 211602, 2018
  21. Characteristic Orientation Relationships in Nanoscale Al-Al2Cu Eutectic, S.J. Wang, G. Liu, J. Wang, A. Misra, Materials Characterization, 142, 170-178, 2018
  22. Plasticity of Laser-Processed Nanoscale Al-Al2Cu Eutectic Alloy, S.J. Wang, G. Liu, D.Y. Xie, Q. Lei, B.P. Ramakrishnan, J. Mazumder, J. Wang, A. Misra, Acta Materialia, 156, 52-63, 2018
  23. High Efficiency Si Photocathode Protected by Multifunctional GaN Nanostructures, S. Vanka, E. Arca, K. Sun, G.A. Botton, G. Teeter, Z. Mi, Nano Letters, 18, 6530-6537, 2018
  24. Effects of Substrate Temperature and Deposition Rate on the Phase Separated Morphology of Co-Sputtered, Cu-Mo Thin Films, B. Derby, Y. Cui, J.K. Baldwin, A. Misra, Thin Solid Films, 647, 50-56, 2018
  25. The Effect of Cold Rolling on Grain Boundary Structure and Stress Corrosion Cracking Susceptibility of Twins in Alloy 690 in Simulated PWR Primary Water Environment, W. Kuang, G.S. Was, C. Miller, M. Kaufman, T. Alam, B. Gwalani, and R. Banerjee, Corrosion Science, 130, 126-137, 2018
  26. Probing Long-Range Ordering in Nickel-Base Alloys with Proton Irradiation, M. Song, Y. Yang, M. Wang, W. Kuang, C.R. Lear, G.S. Was, Acta Materialia, 156, 446-462, 2018
  27. Solar Water Oxidation by an InGaN Nanowire Photoanode with a Bandgap of 1.7 eV, S. Chu , S. Vanka, Y. Wang, J. Gim, Y. Wang, Y. Ra, R. Hovden, H. Guo, I. Shih, Z. Mi, ACS Energy Letters, 3, 307-314, 2018
  28. Deformation Behavior of β’ and β”’ Precipitates in Mg-RE Alloys, E.L.S. Solomon, E.A. Marquis, Materials Letters, 2018
  29. Heteroepitaxy of Fin-Shaped InGaN Nanoridge Using Molecular Beam Epitaxy, Y. Park, J. Gim, R. Yalisove, R. Hovden, Z. Mi, Crystal Growth and Design, 18, 5750-5756, 2018
  30. Molecular Beam Epitaxy and Characterization of Mg-Doped GaN Epilayers Grown on Si (0 0 1) Substrate through Controlled Nanowire Coalescence, Y. Wu, Y. Wang, K. Sun, A. Aiello, P. Bhattacharya, Z. Mi, Journal of Crystal Growth, 498, 109-114, 2018
  31. Characterization of M2X Formed during 5 MeV Fe2+ Irradiation, E. Getto, K. Sun, G.S. Was, Journal of Nuclear Materials, 485, 154-158, 2017
  32. The Oxidation of Alloy 690 in Simulated Pressurized Water Reactor Primary Water, W. Kuang, M. Song, P. Wang, G.S. Was, Corrosion Science, 126, 227-237, 2017
  33. Addressing Challenges and Scalability in the Synthesis of Thin Uniform Metal Shells on Large Metal Nanoparticle Cores: Case Study of Ag-Pt Core-Shell Nanocubes U. Aslam, S. Linic, ACS Applied Materials & Interfaces 9(49), 43127-43132, 2017
  34. Radiation-Induced Segregation on Defect Clusters in Single-Phase Concentrated Solid-Solution Alloys, C. Lu, T. Yang, K. Jin, N. Gao, P. Xiu, Y. Zhang, F. Gao, H. Bei, W.J. Weber, K. Sun, Y. Dong, L.M. Wang, Acta Materialia, 127, 98-107, 2017
  35. Amorphization of Ta2O5 Under Swift Heavy Ion Irradiation, A.B. Cusick, M. Lang, F.X. Zhang, K. Sun, W.X. Li, P. Kluth, C. Trautmann, R.C. Ewing, Nuclear Instruments & Methods in Physics Research B, 407, 25-33, 2017
  36. Indium-Doped Co3O4 Nanorods for Catalytic Oxidation of CO and C3H6 Towards Diesel Exhaust, L. Ma, C.Y. Seo, X.Y. Chen, K. Sun, J.W. Schwank, Applied Catalysis B-Environmental, 222, 44-58, 2017
  37. Effect of Laser Surface Remelting on the Microstructure and Properties of Al-Al2Cu-Si Ternary Eutectic Alloy, B.P. Ramakrishnan, Q. Lei, A. Misra, J. Mazumder, Scientific Reports, 7, 13468, 2017
  38. Enhanced Radiation-Tolerant Oxide Dispersion Strengthened Steel and its Microstructure Evolution under Helium-Implantation and Heavy-Ion Irradiation, C. Lu, Z. Lu, X. Wang, R. Xie, Z. Li, M. Higgins, C. Liu, F. Gao, L. Wang, Scientific Reports, 7, 40343, 2017
  39. In Situ Atomic-Scale Observation of the Two-Dimensional Co(OH)2 Transition at Atmospheric Pressure, X. Shen, S. Dai, C. Zhang, S. Zhang, S.M. Sharkey, G.W. Graham, X. Pan, Z. Peng, Chemistry of Materials, 29, 4572-4579, 2017
  40. Early Precipitate Morphologies in Mg-Nd-(Zr) Alloys, E.L.S. Solomon, V. Araullo-Peters, J.E. Allison, E.A. Marquis, Scripta Materialia, 128, 14-17, 2017
  41. Effect of Y/Ti Atomic Ratio on Microstructure of Oxide Dispersion Strengthened Alloys, C. Lu, Z. Lu, R. Xie, Z. Li, C. Liu, L. Wang, Materials Characterization, 134, 35-40, 2017
  42. Controlling Energy Flow in Multimetallic Nanostructures for Plasmonic Catalysis, U. Aslam, S. Chavez, S. Linic, Nature Nanotechnology, 12, 1000-1005, 2017
  43. Structural Differences between Capped GaSb Nanostructures Grown by Stranski-Krastanov and Droplet Epitaxy Growth Modes, M. DeJarld, L. Yan, M. Luengo-Kovac, V. Sih, J.M. Millunchick, Journal of Applied Physics, 121(3), 34301, 2017
  44. Droplet Induced Compositional Inhomogeneities in GaAsBi, C.R. Tait, L. Yan, J.M. Millunchick, Applied Physics Letters, 111(4), 42105, 2017
  45. High Performance Red-Emitting Multiple Layer InGaN/GaN Quantum Dot Lasers, T. Frost, A. Hazari, A. Aiello, M.Z. Baten, L. Yan, J.M. Millunchick, P. Bhattacharya, Japanese Journal of Applied Physics, 55(3), 32101, 2016
  46. Experimental Evidence of ZnS Precursor Anisotropy Activated by Ethylenediamine for Constructing Nanowires and Single-Atomic Layered Hybrid Structures, S.B. Han, W. Liu, K. Sun, X.T. Zu, CrystEngComm, 8(15), 2626-2631, 2016
  47. Memristive Behavior and Ideal Memristor of 1T phase MoS2 Nanosheets, P.F. Cheng, K. Sun, Y.H. Hu, Nano Letters, 16(1), 572-576, 2016
  48. An Efficient Counter Electrode Material for Dye-Sensitized Solar Cells—Flower-Structured 1T Metallic Phase MoS2, W. Wei, K. Sun, Y.H. Hu, Journal of Materials Chemistry, 4(32), 12398-12401, 2016
  49. Mechanically-Induced Reverse Phase Transformation of MoS2 from Stable 2H to Metastable 1T and its Memristive Behavior, P. Cheng, K. Sun, Y.H. Hu, RSC Advances, 6(70), 65691-65697, 2016
  50. The Bright Future for Electrode Materials of Energy Devices ─ Highly Conductive Porous Na-Embedded Carbon, W. Wei, L. Chang, K. Sun, A. Pak, E. Paek, G. Hwang, Y.H. Hu, Nano Letters, 16(12), 8029-8033, 2016
  51. Enhancing Radiation Tolerance by Controlling Defect Mobility and Migration Pathways in Multicomponent Single-Phase Alloys, C. Lu, L. Niu, N. Chen, K. Jin, T. Yang, P. Xiu, Y. Zhang, F.  Gao, H. Bei, S. Shi, M. He, I.M. Robertson, W.J. Weber, L. Wang, Nature Communications, 7, 13564, 2016
  52. On the Early Stages of Precipitation in Dilute Mg-Nd Alloys, A.R. Natarajan, E.L.S. Solomon, B. Puchala, E.A. Marquis, A. Van der Ven, Acta Materialia, 108, 367-379, 2016
  53. Microstructure of HIPed and SPSed 9Cr-ODS Steel and its Effect on Helium Bubble Formation, C. Lu, Z. Lu, R. Xie, C. Liu, L. Wang, Journal of Nuclear Materials, 474, 65-75, 2016
  54. Direct Observation of Defect Range and Evolution in Ion-Irradiated Single Crystalline Ni and Ni Binary Alloys, C. Lu, K. Jin, L.K. Béland, F. Zhang, T. Yang, L. Qiao, Y. Zhang, H. Bei, H.M. Christen, R.E. Stoller, L. Wang, Scientific Reports, 6, 19994, 2016
  55. Kinetic Trapping of Immisicible Metal Atoms into Bimetallic Nanoparticles through Plasmonic Visible Light-Mediated Reduction of a Bimetallic Oxide Precursor: Case Study of Ag-Pt Nanoparticle Synthesis, U. Aslam, S. Linic, Chemistry of Materials, 28(22), 8289-8295, 2016
  56. Mechanism of Charge Transfer from Plasmonic Nanostructures to Chemically Attached Materials, C. Boerigter, U. Aslam, S. Linic, ACS Nano, 10(6), 6108-6115, 2016
  57. Chemistry and Morphology of b’ Precipitates in an Aged Mg-Nd-Y-Zr Alloy, E. Sitzmann, E.A. Marquis, Phil. Mag. Letters, 95(1), 7-13, 2015 
  58. Polarization-Dependent Raman Spectroscopy of Epitaxial TiO2(B) Thin Films, J.R. Jokisaari, D. Bayerl, K. Zhang, L. Xie, Y. Nie, D.G. Schlom, E. Kioupakis, G.W. Graham, X. Pan, Chemistry of Materials, 27(23), 7896-7902, 2015