Michigan Center for Materials Characterization > Techniques and Instruments > JEOL 3100R05

JEOL 3100R05

Applications

  • Aberration-corrected HAADF/LAADF/ABF/BF STEM imaging for atomic structures
  • Fast EELS mapping with K2 direct electron detector
  • Conventional BF/DF TEM imaging, SAED, and aberration-corrected HRTEM imaging
  • Low-dose TEM and energy-filtered TEM with K2 direct electron detector

Contact

Tao Ma

Location

Room G026 (Microscope) and G028 (Control Room)

Acknowledgments

Publications, presentations, and posters resulting from work on this instrument should state: “The authors acknowledge the financial support of the University of Michigan College of Engineering and NSF grant #DMR-0723032, and technical support from the Michigan Center for Materials Characterization.“

Specifications

  • Accelerating Voltage
    • 80, 200 and 300 kV 
  • Filament
    • Tungsten cold field emission tip
  • Vacuum
    • Gun ~1.0 x 10-9 torr
    • Column ~1.0 x 10-7 torr
  • Resolution
    • CTEM 0.055 nm point-to-point
    • STEM 0.055 nm point-to-point
  • Aberration correctors
    • Evaluate and correct aberrations directly from Ronchigram with an autocorrelation function
    • Auto correction on real samples. No standard sample is required.
  • XEDS System
    • Horizontal Ultra-thin Window JEOL SDD X-ray detector (active area = 60 mm2) capable of detecting elements with Z >5.
  • EELS System
    • Gatan Quantum 969 Imaging Filter (GIF) wtih K2 direct electron detector for electron energy loss spectroscopy and imaging.
  • Image Acquisition & Analysis System
    • Gatan Ultrascan 1000 CCD camera for high resolution imaging (above the GIF)
  • Compatible sample Holders
    • JEOL Single-Tilt Stage
    • JEOL Double-Tilt Analytical Stage
    • Gatan #636 Double-Tilt (x=±35 degrees, y=±35 degrees) Low Background (Be) Liquid-Nitrogen Stage.
    • Gatan #652 Double-Tilt Heating Holder with a maximum operating temperature of 1000 degrees Celsius.
  • In-situ holders
    • Hysitron PI-95 pico-indenter
  • Other Accessories
    • Free lens control, fully independent control of all lenses.
    • TEMCon PC control software.
    • JEOL Cs Correctors for STEM and TEM 

References

  1. Demonstration of Device-Quality 60% Relaxed In0. 2Ga0. 8N on Porous GaN Pseudo-Substrates Grown by PAMBE, C. Wurm, H. Collins, N. Hatui, W. Li, S. Pasayat, R. Hamwey, K. Sun, I. Sayed, K. Khan, E. Ahmadi, S. Keller, U. Mishra, Journal of Applied Physics, 131, 015701, 2022
  2. Quaternary Alloy ScAlGaN: A Promising Strategy to Improve the Quality of ScAlN, P. Wang, D. Wang, Y. Bi, B. Wang, J. Schwartz, R. Hovden, Z. Mi, Applied Physics Letters, 120, 012104, 2022
  3. Observation of Self-Assembled InGaN/GaN Superlattice Structure Grown on N-Polar GaN by Plasma-Assisted Molecular Beam Epitaxy, K. Khan, S. Diez, K. Sun, C. Wurm, U.K. Mishra, E. Ahmadi, APL Materials, 9, 121114, 2021
  4. Large Area Friction Stir Additive Manufacturing of Intermetallic-Free Aluminum-Steel Bimetallic Components through Interfacial Amorphization, F. Liu, Y. Zhang, P. Dong, Journal of Manufacturing Processes, 73, 725-735, 2022
  5. Self-Assembly Mechanism of Complex Corrugated Particles, L. Tang, T. Vo, X. Fan, D. Vecchio, T. Ma, J. Lu, H. Hou, S.C. Glotzer, N.A. Kotov, J. Am. Chem. Soc., 143(47), 19655-19667, 2021
  6. Direct Methane Activation by Atomically Thin Platinum Nanolayers on Two-Dimensional Metal Carbides, Z. Li, Y. Xiao, P.R. Chowdhury, Z. Wu, T. Ma, J.Z. Chen, G. Wan, T-H. Kim, D. Jing, P.J. Potdar, L. Zhou, Z. Zeng, X. Ruan, J.T. Miller, J.P. Greeley, Y. Wu, A. Varma, Nature Catalysis, 4, 882-891, 2021
  7. Fullerene-Functionalized Poly (3-hexylthiophene) Additive Stabilizes Conjugated Polymer–Fullerene Blend Morphologies, D. Kim, E.A. Mueller, D.S. Yang, D.E. Fagnani, J. Kim, A.J. McNeil, ACS Appl. Polym. Mater., 2021
  8. Atomically Dispersed Pb Ionic Sites in PbCdSe Quantum Dot Gels Enhance Room-Temperature NO2 Sensing, X. Geng, S. Li, L. Mawella-Vithanage, T. Ma, M. Kilani, B. Wang, L. Ma, C.C. Hewa-Rahinduwage, A. Shafikova, E. Nikolla, G. Mao, S.L. Brock, L. Zhang, L. Luo, Nature Communications, 12, 4895, 2021
  9. Stable and Selective Catalysts for Propane Dehydrogenation Operating at Thermodynamic limit, A.H. Motagamwala, R. Almallahi, J. Wortman, V.O. Igenegbai, S. Linic, Science, 373(6551), 217-222
  10. Quantum Dot Assembly Driven by Electrochemically Generated Metal-Ion Crosslinkers, C.C. Hewa-Rahinduwage, K.L. Silva, S.L. Brock, L. Luo, Chemistry of Materials, 33(12), 4522-4528, 2021
  11. Engineering New Limits to Magnetostriction Through Metastability in Iron-Gallium Alloys, P.B. Meisenheimer, R.A. Steinhardt, S.H. Sung, L.D. Williams, S. Zhuang, M.E. Nowakowski, S. Novakov, M.M. Torunbalci, B. Prasad, C.J. Zollner, Z. Wang, N.M. Dawley, J. Schubert, A.H. Hunter, S. Manipatruni, D.E. Nikonov, I.A. Young, L.Q. Chen, J. Bokor, S.A. Bhave, R. Ramesh, J.-M. Hu, E. Kioupakis, R. Hovden, D.G. Schlom, J.T. Heron, Nature Communications, 12, 2757, 2021
  12. Hierarchical Microstructures and Deformation Behavior of Laser Direct-Metal-Deposited Cu-Fe Alloys, A. Chatterjee, E. Sprague, J. Mazumder, A. Misra, Materials Science and Engineering A, 802, 140659, 2021
  13. From Thick Intermetallic to Nanoscale Amorphous Phase at Al-Fe Joint Interface: Roles of Friction Stir Welding Conditions, F.C. Liu, P. Dong, Scripta Materialia, 191, 167-172, 2021
  14. Distribution of Transition Metal Elements in an Al-Si-Cu-Based Alloy, Q. Shi, Y. Huo, T. Berman, B. Ghaffri, M. Lei, J. Allison, Scripta Materialia, 190, 97-102, 2021
  15. Fracture Resistance of Hierarchical Cu–Mo Nanocomposite Thin Films, Y. Cui, B. Derby, N. Li, A. Misra, Materials Science and Engineering A, 799, 139891, 2021
  16. Microstructure and Mechanical Properties of Nanoscale Cu/(Ta50Nb25Mo25) Multilayers, L. Jiang, M. Powers, Y. Cui, B.K. Derby, A. Misra, Materials Science and Engineering A, 799, 140200, 2021
  17. Controlling Defect Formation of Nanoscale AlN: Toward Efficient Current Conduction of Ultrawide‐Bandgap Semiconductors, Y. Wu, D.A. Laleyan, Z. Deng, C. Ahn, A.F. Aiello, A. Pandey, X. Liu, P. Wang, K. Sun, E. Ahmadi, Y. Sun, M. Kira, P.K. Bhattacharya, E. Kioupakis, Z. Mi, Advanced Electronic Materials, 6(9), 2020
  18. Optimal STEM Convergence Angle Selection using a Convolutional Neural Network and the Strehl Ratio, N. Schnitzer, S.H. Sung, R. Hovden, Microscopy and Microanalysis, 26(5), 921-928, 2020
  19. Metal-Ion-Controlled Growth and Nanoindentation Response of 3D, Bicontinuous Cu–Fe Thin Films, B.K. Derby, A. Chatterjee, A. Misra, Journal of Applied Physics, 128, 035303, 2020
  20. Alloy Amorphization through Nanoscale Shear Localization at Al-Fe Interface, F.C. Liu, P. Dong, J. Zhang, W. Lu, A. Taub, K. Sun, Materials Today Physics, 15, 100252, 2020
  21. Influence of Quantum Dot Morphology on the Optical Properties of GaSb/GaAs Multilayers, C. Greenhill, A.S. Chang, E.S. Zech, S. Clark, G. Balakrishnan, R.S. Goldman, Applied Physics Letters, 116, 252107, 2020
  22. Multi-Step Crystallization of Self-Organized Spiral Eutectics, S. Moniri, H. Bale, T. Volkenandt, Y. Wang, J. Gao, T. Lu, K. Sun, R.O. Richie, A.J. Shahani, Small, 1906146, 2020
  23. Performance Characteristics of AlGaN Tunnel Junction Light Emitting Diodes, A. Pandey, W. Shin, R. Hovden, Z. Mi, Photonics Research, 8(3), 331-337, 2020
  24. Self-Assembly of Chiral Nanoparticles into Semiconductor Helices with Tunable Near-Infrared Optical Activity, J. Yan, W. Feng, J-Y. Kim, J. Lu, P. Kumar, Z. Mu, X. Wu, X. Mao, N.A. Kotov, Chem. Mater., 32(1), 476-488, 2020 
  25. Monolayer GaN Excitonic Deep Ultraviolet Light Emitting Diodes, Y. Wu, X. Liu, P. Wang, D.A. Laleyan, K. Sun, Y. Sun, C. Ahn, M. Kira, E. Kioupakis, Z. Mi, Applied Physics Letters, 116, 013101, 2020 
  26. Monolithic Integration of High-Voltage Thin-Film Electronics on Low-Voltage Integrated Circuits Using a Solution Process, Y. Son, B. Frost, Y. Zhao, R.L. Peterson, Nature Electronics, 2, 540-548, 2019
  27. Influence of Metal Nanocomposite Morphology on Helium Implantation Response, B.K. Derby, J.K. Baldwin, Y. Wang, M.J. Demkowicz, A. Misra, N. Li, Scripta Materialia, 177, 229-233, 2019
  28. Faceted He-Filled “Pancakes” Confined within Nanoscale Metal Layers, B.K. Derby, J.K. Baldwin, D. Chen, M.J. Demkowicz, Y.Q. Wang, A. Misra, N. Li, JOM, 1-5, 2019
  29. Nanoscale Deformation Mechanics Reveal Resilience in Nacre of Pinna Nobilis Shell, J. Gim, N. Schnitzer, L.M. Otter, Y. Cui, S. Motreuil, F. Marin, S.E. Wolf, D.E. Jacob, A. Misra, R. Hovden, Nature Communications, 10, 4822, 2019
  30. A Single-Junction Cathodic Approach for Stable Unassisted Solar Water Splitting, Y. Wang, Y. Wu, J. Schwartz, S. Sung, R. Hovden, Z. Mi, Joule, 3(10), 2444-2456, 2019 
  31. Tuning Catalytic Performance by Controlling Reconstruction Process in Operando Condition, C. Cai, S. Han, K. Sun, L. Qiao, S. Li, X. Zu, Applied Catalysis B: Environmental, 260, 118103, 2019
  32. Stable Unassisted Solar Water Splitting on Semiconductor Photocathodes Protected by Multi-Functional GaN Nanostructures, Y. Wang, J. Schwartz, J. Gim, R. Hovden, Z. Mi, ACS Energy Letters, 4, 1541-1548, 2019
  33. A Quadruple-Band Metal-Nitride Nanowire Artificial Photosynthesis System for High Efficiency Photocatalytic Overall Solar Water Splitting, Y. Wang, Y. Wu, K. Sun, Z. Mi, Materials Horizons, 2019
  34. Stability and Strain-Driven Evolution of β′ Precipitate in Mg-Y Alloys, E.L.S. Solomon, A.R. Natarajan, A.M. Roy, V. Sundararaghavan, A. Van der Ven, E.A. Marquis, Acta Materialia, 166, 148-157, 2019
  35. Design of Bicontinuous Metallic Nanocomposites for High-Strength and Plasticity, Y. Cui, B. Derby, N. Li, A. Misra, Materials Design, 166, 107602, 2019
  36. Dislocation Pile-Ups at β1 Precipitate Interfaces in Mg-Rare Earth (RE) Alloys, Z. Huang, C. Yang, L. Qi, J.E. Allison, A. Misra, Materials Science & Engineering A, 742, 278-286, 2019
  37. An In0.42Ga0.58N Tunnel Junction Nanowire Photocathode Monolithically Integrated on a Nonplanar Si Wafer, Y. Wang, S. Vanka, J. Gim, Y. Wu, R. Fan, Y. Zhang, J. Shi, M. Shen, R. Hovden, Z. Mi, Nano Energy, 57, 405-413, 2019
  38. Optical and Interface Characteristics of Al0.56Ga0.44N/Al0.62Ga0.38N Multiquantum Wells with ∼280 nm Emission Grown by Plasma-Assisted Molecular Beam Epitaxy, Journal of Crystal Growth, 508, 66-71, 2019
  39. Processing of Novel Pseudomorphic Cu–Mo Hierarchies in Thin Films, B. Derby, Y. Cui, J. Baldwin, R. Arróyave, M.J. Demkowicz, A. Misra, Materials Research Letters, 7(1), 1-11, 2018
  40. Suppression of Shear Banding in High-Strength Cu/Mo Nanocomposites with Hierarchical Bicontinuous Intertwined Structures, Y. Cui, B. Derby, N. Li, N.A. Mara, A. Misra, Materials Research Letters, 6(3), 184-190, 2018
  41. Surfactant-Induced Chemical Ordering of GaAsN:Bi, J. Occena, T. Jen, H. Lu, B.A. Carter, T.S. Jimson, A.G. Norman, R.S. Goldman, Applied Physics Letters, 113, 211602, 2018
  42. Characteristic Orientation Relationships in Nanoscale Al-Al2Cu Eutectic, S.J. Wang, G. Liu, J. Wang, A. Misra, Materials Characterization, 142, 170-178, 2018
  43. Plasticity of Laser-Processed Nanoscale Al-Al2Cu Eutectic Alloy, S.J. Wang, G. Liu, D.Y. Xie, Q. Lei, B.P. Ramakrishnan, J. Mazumder, J. Wang, A. Misra, Acta Materialia, 156, 52-63, 2018
  44. High Efficiency Si Photocathode Protected by Multifunctional GaN Nanostructures, S. Vanka, E. Arca, K. Sun, G.A. Botton, G. Teeter, Z. Mi, Nano Letters, 18, 6530-6537, 2018
  45. Effects of Substrate Temperature and Deposition Rate on the Phase Separated Morphology of Co-Sputtered, Cu-Mo Thin Films, B. Derby, Y. Cui, J.K. Baldwin, A. Misra, Thin Solid Films, 647, 50-56, 2018
  46. The Effect of Cold Rolling on Grain Boundary Structure and Stress Corrosion Cracking Susceptibility of Twins in Alloy 690 in Simulated PWR Primary Water Environment, W. Kuang, G.S. Was, C. Miller, M. Kaufman, T. Alam, B. Gwalani, and R. Banerjee, Corrosion Science, 130, 126-137, 2018
  47. Probing Long-Range Ordering in Nickel-Base Alloys with Proton Irradiation, M. Song, Y. Yang, M. Wang, W. Kuang, C.R. Lear, G.S. Was, Acta Materialia, 156, 446-462, 2018
  48. Solar Water Oxidation by an InGaN Nanowire Photoanode with a Bandgap of 1.7 eV, S. Chu , S. Vanka, Y. Wang, J. Gim, Y. Wang, Y. Ra, R. Hovden, H. Guo, I. Shih, Z. Mi, ACS Energy Letters, 3, 307-314, 2018
  49. Deformation Behavior of β’ and β”’ Precipitates in Mg-RE Alloys, E.L.S. Solomon, E.A. Marquis, Materials Letters, 2018
  50. Heteroepitaxy of Fin-Shaped InGaN Nanoridge Using Molecular Beam Epitaxy, Y. Park, J. Gim, R. Yalisove, R. Hovden, Z. Mi, Crystal Growth and Design, 18, 5750-5756, 2018
  51. Molecular Beam Epitaxy and Characterization of Mg-Doped GaN Epilayers Grown on Si (0 0 1) Substrate through Controlled Nanowire Coalescence, Y. Wu, Y. Wang, K. Sun, A. Aiello, P. Bhattacharya, Z. Mi, Journal of Crystal Growth, 498, 109-114, 2018
  52. Characterization of M2X Formed during 5 MeV Fe2+ Irradiation, E. Getto, K. Sun, G.S. Was, Journal of Nuclear Materials, 485, 154-158, 2017
  53. The Oxidation of Alloy 690 in Simulated Pressurized Water Reactor Primary Water, W. Kuang, M. Song, P. Wang, G.S. Was, Corrosion Science, 126, 227-237, 2017
  54. Addressing Challenges and Scalability in the Synthesis of Thin Uniform Metal Shells on Large Metal Nanoparticle Cores: Case Study of Ag-Pt Core-Shell Nanocubes U. Aslam, S. Linic, ACS Applied Materials & Interfaces 9(49), 43127-43132, 2017
  55. Radiation-Induced Segregation on Defect Clusters in Single-Phase Concentrated Solid-Solution Alloys, C. Lu, T. Yang, K. Jin, N. Gao, P. Xiu, Y. Zhang, F. Gao, H. Bei, W.J. Weber, K. Sun, Y. Dong, L.M. Wang, Acta Materialia, 127, 98-107, 2017
  56. Amorphization of Ta2O5 Under Swift Heavy Ion Irradiation, A.B. Cusick, M. Lang, F.X. Zhang, K. Sun, W.X. Li, P. Kluth, C. Trautmann, R.C. Ewing, Nuclear Instruments & Methods in Physics Research B, 407, 25-33, 2017
  57. Indium-Doped Co3O4 Nanorods for Catalytic Oxidation of CO and C3H6 Towards Diesel Exhaust, L. Ma, C.Y. Seo, X.Y. Chen, K. Sun, J.W. Schwank, Applied Catalysis B-Environmental, 222, 44-58, 2017
  58. Effect of Laser Surface Remelting on the Microstructure and Properties of Al-Al2Cu-Si Ternary Eutectic Alloy, B.P. Ramakrishnan, Q. Lei, A. Misra, J. Mazumder, Scientific Reports, 7, 13468, 2017
  59. Enhanced Radiation-Tolerant Oxide Dispersion Strengthened Steel and its Microstructure Evolution under Helium-Implantation and Heavy-Ion Irradiation, C. Lu, Z. Lu, X. Wang, R. Xie, Z. Li, M. Higgins, C. Liu, F. Gao, L. Wang, Scientific Reports, 7, 40343, 2017
  60. In Situ Atomic-Scale Observation of the Two-Dimensional Co(OH)2 Transition at Atmospheric Pressure, X. Shen, S. Dai, C. Zhang, S. Zhang, S.M. Sharkey, G.W. Graham, X. Pan, Z. Peng, Chemistry of Materials, 29, 4572-4579, 2017
  61. Early Precipitate Morphologies in Mg-Nd-(Zr) Alloys, E.L.S. Solomon, V. Araullo-Peters, J.E. Allison, E.A. Marquis, Scripta Materialia, 128, 14-17, 2017
  62. Effect of Y/Ti Atomic Ratio on Microstructure of Oxide Dispersion Strengthened Alloys, C. Lu, Z. Lu, R. Xie, Z. Li, C. Liu, L. Wang, Materials Characterization, 134, 35-40, 2017
  63. Controlling Energy Flow in Multimetallic Nanostructures for Plasmonic Catalysis, U. Aslam, S. Chavez, S. Linic, Nature Nanotechnology, 12, 1000-1005, 2017
  64. Structural Differences between Capped GaSb Nanostructures Grown by Stranski-Krastanov and Droplet Epitaxy Growth Modes, M. DeJarld, L. Yan, M. Luengo-Kovac, V. Sih, J.M. Millunchick, Journal of Applied Physics, 121(3), 34301, 2017
  65. Droplet Induced Compositional Inhomogeneities in GaAsBi, C.R. Tait, L. Yan, J.M. Millunchick, Applied Physics Letters, 111(4), 42105, 2017
  66. High Performance Red-Emitting Multiple Layer InGaN/GaN Quantum Dot Lasers, T. Frost, A. Hazari, A. Aiello, M.Z. Baten, L. Yan, J.M. Millunchick, P. Bhattacharya, Japanese Journal of Applied Physics, 55(3), 32101, 2016
  67. Experimental Evidence of ZnS Precursor Anisotropy Activated by Ethylenediamine for Constructing Nanowires and Single-Atomic Layered Hybrid Structures, S.B. Han, W. Liu, K. Sun, X.T. Zu, CrystEngComm, 8(15), 2626-2631, 2016
  68. Memristive Behavior and Ideal Memristor of 1T phase MoS2 Nanosheets, P.F. Cheng, K. Sun, Y.H. Hu, Nano Letters, 16(1), 572-576, 2016
  69. An Efficient Counter Electrode Material for Dye-Sensitized Solar Cells—Flower-Structured 1T Metallic Phase MoS2, W. Wei, K. Sun, Y.H. Hu, Journal of Materials Chemistry, 4(32), 12398-12401, 2016
  70. Mechanically-Induced Reverse Phase Transformation of MoS2 from Stable 2H to Metastable 1T and its Memristive Behavior, P. Cheng, K. Sun, Y.H. Hu, RSC Advances, 6(70), 65691-65697, 2016
  71. The Bright Future for Electrode Materials of Energy Devices ─ Highly Conductive Porous Na-Embedded Carbon, W. Wei, L. Chang, K. Sun, A. Pak, E. Paek, G. Hwang, Y.H. Hu, Nano Letters, 16(12), 8029-8033, 2016
  72. Enhancing Radiation Tolerance by Controlling Defect Mobility and Migration Pathways in Multicomponent Single-Phase Alloys, C. Lu, L. Niu, N. Chen, K. Jin, T. Yang, P. Xiu, Y. Zhang, F.  Gao, H. Bei, S. Shi, M. He, I.M. Robertson, W.J. Weber, L. Wang, Nature Communications, 7, 13564, 2016
  73. On the Early Stages of Precipitation in Dilute Mg-Nd Alloys, A.R. Natarajan, E.L.S. Solomon, B. Puchala, E.A. Marquis, A. Van der Ven, Acta Materialia, 108, 367-379, 2016
  74. Microstructure of HIPed and SPSed 9Cr-ODS Steel and its Effect on Helium Bubble Formation, C. Lu, Z. Lu, R. Xie, C. Liu, L. Wang, Journal of Nuclear Materials, 474, 65-75, 2016
  75. Direct Observation of Defect Range and Evolution in Ion-Irradiated Single Crystalline Ni and Ni Binary Alloys, C. Lu, K. Jin, L.K. Béland, F. Zhang, T. Yang, L. Qiao, Y. Zhang, H. Bei, H.M. Christen, R.E. Stoller, L. Wang, Scientific Reports, 6, 19994, 2016
  76. Kinetic Trapping of Immisicible Metal Atoms into Bimetallic Nanoparticles through Plasmonic Visible Light-Mediated Reduction of a Bimetallic Oxide Precursor: Case Study of Ag-Pt Nanoparticle Synthesis, U. Aslam, S. Linic, Chemistry of Materials, 28(22), 8289-8295, 2016
  77. Mechanism of Charge Transfer from Plasmonic Nanostructures to Chemically Attached Materials, C. Boerigter, U. Aslam, S. Linic, ACS Nano, 10(6), 6108-6115, 2016
  78. Chemistry and Morphology of b’ Precipitates in an Aged Mg-Nd-Y-Zr Alloy, E. Sitzmann, E.A. Marquis, Phil. Mag. Letters, 95(1), 7-13, 2015 
  79. Polarization-Dependent Raman Spectroscopy of Epitaxial TiO2(B) Thin Films, J.R. Jokisaari, D. Bayerl, K. Zhang, L. Xie, Y. Nie, D.G. Schlom, E. Kioupakis, G.W. Graham, X. Pan, Chemistry of Materials, 27(23), 7896-7902, 2015